CA2709402A1 - Composite passive materials for ultrasound transducers - Google Patents

Composite passive materials for ultrasound transducers Download PDF

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Publication number
CA2709402A1
CA2709402A1 CA2709402A CA2709402A CA2709402A1 CA 2709402 A1 CA2709402 A1 CA 2709402A1 CA 2709402 A CA2709402 A CA 2709402A CA 2709402 A CA2709402 A CA 2709402A CA 2709402 A1 CA2709402 A1 CA 2709402A1
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CA
Canada
Prior art keywords
transducer
layer
active acoustic
transducer array
passive layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2709402A
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French (fr)
Inventor
Alain Sadaka
Jian R. Yuan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Boston Scientific Scimed Inc
Original Assignee
Alain Sadaka
Jian R. Yuan
Boston Scientific Scimed, Inc.
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Filing date
Publication date
Application filed by Alain Sadaka, Jian R. Yuan, Boston Scientific Scimed, Inc. filed Critical Alain Sadaka
Publication of CA2709402A1 publication Critical patent/CA2709402A1/en
Abandoned legal-status Critical Current

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Classifications

    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K11/00Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/004Mounting transducers, e.g. provided with mechanical moving or orienting device
    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K11/00Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/02Mechanical acoustic impedances; Impedance matching, e.g. by horns; Acoustic resonators
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/42Piezoelectric device making

Abstract

Provided herein are composite passive layers for ultrasound transducers having acoustic properties that can be easily tailored to the needs of the transducer application using current micro fabrication techniques. In an em-bodiment, a passive layer comprises metal posts (633a, 633b) embedded in a polymer matrix or other material (637). The acoustic properties of the passive layer depend on the metal/polymer volume fraction of the passive layer, which can be easily controlled using current micro fabrication techniques, e.g., integrated circuit (IC) fabrication techniques. Further, the embedded metal posts provide electrical conduction through the passive layer allowing electrical con-nections to be made to an active element, e.g., piezoelectric element (610a, 610b), of the transducer through the passive layer. Because the embedded metal posts conduct along one line of direction, they can be used to provide separate electrical connections to different active elements in a transducer array through the passive layer.

Description

COMPOSITE PASSIVE MATERIALS FOR ULTRASOUND TRANSDUCERS
CROSS-REFERENCE TO RELATED APPLICATIONS
This application claims priority from U.S. Serial No. 11/959,104; filed on December 18, 2007, which is hereby incorporated by reference in its entirety.
FIELD OF THE INVENTION
The present invention relates to ultrasound transducers, and more particularly to composite passive materials for ultrasound transducers.
BACKGROUND INFORMATION
An ultrasound transducer is typically fabricated as a stack of multiple layers that depend on the application of the transducer. Figures la and lb show typical ultrasound transducers. Each transducer comprises, from the bottom up, a backing layer 30, a bottom electrode layer 17, an active element layer (e.g., piezoelectric element or PZT) 10, a top electrode layer 13, a matching layer (or multiple matching layers) 20, and a lens layer (for focused transducers) 35 and 45. The lens may be a convex lens 35 or a concave lens 45. The backing, matching and lens layers are all passive materials that are used to improve and optimize the performance of the transducer. The backing layer is used to attenuate ultrasound energy propagating from the bottom of the transducer so that ultrasound emissions are directed from the top of the transducer and the matching layer is used to enhance acoustic coupling between the transducer and surrounding environment. Different transducer designs (different sizes, frequencies, applications, etc.) require passive materials with different acoustic properties. Therefore, there is a need for effective methods to control the acoustic properties of these materials to deliver consistent performance while maintaining manufacturability and compliance with processing methods.
A common method to control the properties of passive layers is to add different fillers in different quantities to an epoxy or polymer to create a matrix. Common filler materials include tungsten, alumina, and silver (e.g., in powder form). For example, silver is used in very high quantities to make an otherwise insulating epoxy conductive.
Tungsten and alumina are used to control the acoustic impedance of the passive layer by varying the filler/epoxy matrix density. Although the method of using fillers has several advantages in terms of flexibility, simplicity and cost, it also has several drawbacks. This method can only raise the acoustic. impedance up to a certain point after which the epoxy saturates and will not mix with any additional filler. Also, the filler can move around in the epoxy before the epoxy is cured, making it difficult to control the final distribution of the filler in the epoxy.
Another drawback with tungsten and alumina is that the composite material remains nonconductive. Another drawback is that changing the composition of the passive layers in many cases also affects their manufacturability.
Some of these drawbacks can be overcome by adding more processing steps or using novel mixing, casting and fabrication techniques. However, these techniques eliminate the main advantage of using filer/epoxy matrices, which is simplicity and flexibility.
Therefore, there is a need for passive layers and fabrication methods that provide high flexibility and manufacturability without sacrificing performance or cost.
SUMMARY OF THE INVENTION
Provided herein are composite passive layers for ultrasound transducers having acoustic properties that can be easily tailored to the needs of the transducer application using current micro fabrication techniques.
In an embodiment, a passive layer comprises metal posts embedded in a polymer matrix or other material. The acoustic properties of the passive layer depend on the metal/polymer volume fraction of the passive layer, which can be easily controlled using current microfabrication techniques, e.g., integrated circuit (IC) fabrication techniques.
Further, the metal posts provide electrical conduction through the passive layer allowing electrical connections to be made to an active element, e.g., piezoelectric element, of the transducer through the passive layer. Because the embedded metal posts in the example embodiment conduct along one line of direction, they can be used to provide separate electrical connections to different active elements in a transducer array through the passive layer.
In an embodiment, a passive layer is fabricated by applying a photoresist, e.g., using spin coating. Spin coating allows the thickness of the photoresist to be precisely controlled by varying the viscosity of the photoresist and spin parameters. The photoresist is then exposed to UV light through a mask to transfer a pattern from the mask to the photoresist. Portions of the photoresist are then selectively removed, e.g., using a developer, based on the pattern.
Metal is then deposited in the areas where the photoresist has been removed to form the metal posts of the passive layer. Because the spacing, arrangement, and dimensions of the metal posts can be precisely controlled by the mask pattern, this fabrication method allows the meta/polymer fraction volume, and hence acoustic properties of the passive layer to be easily controlled.
Other systems, methods, features and advantages of the invention will be or will become apparent to one with skill in the art upon examination of the following figures and detailed description. It is intended that all such additional systems, methods, features and advantages be included within this description, be within the scope of the invention, and be protected by the accompanying claims.
BRIEF DESCRIPTION OF THE FIGURES
In order to better appreciate the above recited and other advantages of the present inventions are objected, a more particular description of the invention briefly described above will be rendered by reference to specific embodiments thereof, which are illustrated in the accompanying drawings. It should be noted that the components in the figures are not necessarily to scale, emphasis instead being placed upon illustrating the principles of the invention. Moreover, in the figures, like reference numerals designate corresponding parts throughout the different views. However, like parts do not always have like reference numerals. Moreover, all illustrations are intended to convey concepts, where relative sizes, shapes and other detailed attributes may be illustrated schematically rather than literally or precisely.
Fig. 1 a shows a prior art ultrasound transducer comprising of a stack of layers with a convex lens.
Fig. lb shows a prior art ultrasound transducer comprising of a stack of layers with a convex lens.
Fig. 2 shows a transducer according to an exemplary embodiment of the present invention.
Fig. 3 shows a transducer according to another exemplary embodiment of the present invention.
Fig. 4 shows a transducer according to yet another exemplary embodiment of the present invention.
Figs. 5a-5e show process steps for fabricating a transducer according to an exemplary embodiment of the present invention.
Fig. 6 shows a lead connected to a transducer according to an exemplary embodiment of the present invention.
Fig. 7 shows an exploded view of a transducer array according to an exemplary embodiment of the present invention.
Fig. 8 shows an exploded view of a transducer array according to another exemplary embodiment of the present invention.
DETAILED DESCRIPTION
Figure 2 shows an exemplary ultrasound transducer 105 according to an embodiment of the invention. The transducer 105 comprises an active element 110, e.g., a piezoelectric element, and top and bottom electrodes 113 and 117 deposited on the top and bottom surfaces of the active element 110, respectively. The electrodes 113 and 117 may comprise thin layers of gold, chrome, or other conductive material. The transducer's emitting face may have a square shape, circular shape, or other shape.
The transducer 105 further comprises a matching layer 120 on top of the active element 110. The matching layer 120 comprises a plurality of metallic posts 123 embedded in a polymer matrix 127 or other material. The acoustic properties of the matching layer 120 depend on the metal/polymer volume fraction of the matching layer 120.
Generally, the acoustic impedance increases for increases in the volume fraction of metal.
For other materials, the acoustic properties depend on the metal/material volume fraction, where the material is the material in which the metal posts are embedded. As discussed below, the metal/polymer volume fraction can be easily controlled using current microfabrication techniques, e.g., IC and MEMS fabrication techniques. Because the metal/polymer volume fraction can be easily controlled, the acoustic properties of the matching layer 120 can be easily tailored to the needs of the transducer application using current fabrication techniques.
The transducer 105 also comprises a backing layer 130 underneath the active element 110.
Figure 3 shows an exemplary ultrasound transducer 205 according to another embodiment of the invention. Similar to the previous embodiment, the transducer 205 comprises an active element 110, e.g., piezoelectric element, and top and bottom electrodes 113 and 117 deposited on the top and bottom of the active element 110, respectively. The transducer 205 also comprises a matching layer 220 on top of the active element 110.
The transducer 205 further comprises a backing layer 230 underneath the active element. The backing layer 230 comprises a plurality of metallic posts 233 embedded in a polymer matrix 237 or other material. The acoustic properties of the backing layer 230 depend on the metal/polymer volume fraction of the backing layer 230, which can be easily controlled using current microfabrication techniques, e.g., IC and MEMS
fabrication techniques.
Figure 4 shows an exemplary ultrasound transducer according to yet another embodiment of the invention. In this embodiment, the matching layer 320 comprises a plurality of metallic posts 323 embedded in a polymer matrix 327 or other material. Similarly, the backing layer 330 comprises a plurality of metallic posts 333 embedded in a polymer matrix 337 or other material.
Processing steps for fabricating a transducer according to an exemplary embodiment will now be given with reference to Figures 5(a)-5(e). In this example, a matching layer is fabricated on the active element. However, it is to be understood that the processing steps can also be used to fabricate the backing layer or other passive layers of the transducer.
Figure 5(a) shows an active element 110, e.g., a piezoelectric element, with top and bottom electrodes 113 and 117, e.g., gold on chrome electrodes.
In Figure 5(b) a layer of light-sensitive polymer or epoxy 427 is applied on top of the active element 110 using spin or spray coating. Other coating processes may also be used. In this example, spin coating is used to apply the layer of light-sensitive polymer or epoxy 427.
The polymer or epoxy may be mixed with precursors and solvents to obtain a desired thickness. By varying the polymer or epoxy viscosity and the spin parameters, the coat thickness can be precisely controlled. Most light-sensitive epoxies and polymers are known as photoresists (e.g., UV cured epoxies) and they are classified as either positive or negative based on their response to light. Positive photoresist becomes weaker and more soluble when exposed to light while negative photoresist becomes stronger and less soluble when exposed to light. Photoresists are commonly used in IC and MEMS fabrication with consistent repeatable results.
In Figure 5(c), a mask 460, e.g., chrome on glass, is used in conjunction with light exposure equipment to form a pattern in the photoresist 427. In this example, the photoresist 427 is positive and the mask 460 is transparent 462 in areas where the photoresist 427 is to be removed. UV light 465 is filtered through the mask 460 and reaches the underlying photoresist 427. The areas of the photoresist 427 corresponding to the transparent areas 462 of the mask 460 are exposed to the UV light 465. For the example of negative photoresist, the mask would be opaque in areas where the photoresist is to be removed.
In Figure 5(d), the areas of the photoresist 427 that were exposed to light are removed with a developer, e.g., solvent, leaving the desired pattern imprinted in the photoresist 427. In Figure 5(e), the metal posts 423 are deposited on top of the active element 110 in the areas where the photoresist 427 has been removed. The metal posts 423 may be deposited using sputtering, electroplating, or other metal deposition method. The metal may be nickel, silver, or other conductive material. The photoresist 427 and embedded metal posts 423 form the matching layer 420.

The acoustic properties of the matching layer 420 depend on the metal/polymer volume fraction of the matching layer 420. Because the spacing, arrangement and dimensions of the metal posts 423 can be tightly controlled using the above process steps, the metal/polymer fraction can be tightly controlled to obtain the desired acoustic properties of the matching layer 420 and optimize the transducer design. The pattern (opaque and transparent areas) of the mask determines the spacing, arrangement and dimensions of the metal posts, and hence the metal/polymer volume fraction. The above process can also be used to fabricate the backing layer to control the acoustic properties of the backing layer, and other passive layers to control their acoustic properties.
Therefore, the above process provides an effective method to customize the acoustic properties of passive layers for a particular transducer application. Further, the above process is compatible with current fabrication methods, e.g. IC and MEMS fabrication methods.
Instead of the passive layer comprising the photoresist, the photoresist may be removed, e.g., stripped off, after the metal posts are deposited. A polymer or epoxy may then be applied around the metal post to form the passive layer. For the example of epoxy, the epoxy may be applied around the metal posts, then cured and ground down to the desired passive layer thickness.
Other materials may be used to form the posts besides metal, including nonconductive materials such as oxide, nitride, and the like. In this example, the acoustic properties of the passive layer depends on the volume fraction of the post material to the polymer, e.g., photoresist, in the passive layer.
Metal posts embedded in a polymer matrix not only control the acoustic properties of the passive layer, but also make the passive layer conductive along one direction. A
conductive passive layer is advantageous in an ultrasound transducer because it simplifies the electrical connections of the positive and/or negative leads to the active element.
Figure 6 shows an example of a lead 510 electrically connected to the bottom of the active element 110 through the backing layer 230, which comprises metal posts embedded in a polymer matrix 237. In this example, the lead 510 may be connected to the backing layer 230, e.g., by a conductive epoxy or solder 515, or laser fused to the backing layer. A thin electrode layer 520 may be deposited on the bottom of the backing layer 230 to facilitate the electrical connection. The lead 510 may be part of a twisted pair wire or connected at the other end to a coaxial cable. A lead (not shown) may similarly be electrically connected to the active element through the matching layer. Alternatively, a portion of the matching layer may be removed to expose a small area of the top electrode 113, and the lead (not shown) connected directly to the top electrode 113.
Because the metal posts embedded in the polymer matrix are conductive along one direction (thickness direction), the metal post can be used to provide separate electrical connections to different active elements in a transducer array. This is advantageous over silver based conductive epoxy, which cannot provide separate electrical connections.
The ability of the metal posts to provide separate electrical connection in a transducer array is illustrated in Figure 7. Figure 7 shows an exploded view of an exemplary transducer array comprising two concentric active elements 610a and 610b, e.g., piezoelectric elements PZTs. The transducer array may have more than two active elements.
The transducer array further comprises two electrodes 617a and 617b on the bottom of the active elements 610a and 610b, respectively. The electrodes 617a and 617b are electrically isolated from each other and may comprise thin layers of gold, chrome, or other metal deposited on the active elements. The transducer array further comprises a backing layer 630 comprising metal posts 633a and 633b embedded in a polymer matrix 637. The metal posts 633b are aligned with the electrode 617b while the other metal posts 633a are aligned with the electrode 617a. The number and arrangement of the metal posts shown in Figure 7 are exemplary only. The backing layer 630 may comprise any number of posts in different arrangements. Further, the posts may have different shapes than the ones shown in Figure 7.
The transducer array also comprises electrodes 640a and 640b on the bottom of the backing layer 630. The electrodes 640a and 640b may be connected to separate leads 650a and 650b, respectively, by conductive epoxy, solder, or the like. The electrode 640b aligns with metal posts 633b and electrode 617b while the electrode 640a aligns with metal posts 633a and electrode 617a. Thus, the electrode 640b provides an electrical connection to active element 610b through metal posts 633b and electrode 617b while the electrode 640a provides an electrical connection to active element 610a through metal posts 633a and electrode 617a.
Therefore, the embedded metal posts 633a and 633b enable separate electrical connections to different active elements 610a and 610b in the transducer array through the passive layer 630.
The same principle may be applied to the matching layer (not shown in Figure 7) to provide separate electrical connections through the matching layer. The separate electrical connections provided by the metal post allow the active elements in a transducer array to be independently controlled and driven.

A passive layer comprising embedded metal posts can be used in other transducer arrays having different configurations and sizes depending on the application of the array.
Examples of transducer arrays include linear and annular transducer arrays, two dimensional transducer arrays, and the like.
The advantages that transducers arrays provide in performance and beam manipulation generally come at the price of more complex electronics and controls for coordinating and driving the separate elements of the arrays. Figure 8 shows an exploded view of an exemplary transducer array, in which electronics for controlling the elements of the array are provided near the transducer array. The transducer array in Figure 8 is similar to the one in Figure 7 except for an integrated circuit (IC) chip 710 connected to the bottom electrodes 640a and 640b of the backing layer 630. The IC chip 710 comprises metal contact pads 720a and 720b that align with electrodes 640a and 640b, respectively. The electrodes 640a and 640b may be bonded to the metal contact pads 720a and 720b, respectively, e.g., using solder bumps, to electrically connect the IC chip 710 to the transducer array. The IC
chip 710 also comprises a metal contact pad 730 to connect the IC chip 710 to an ultrasound system via a cable, twisted pair wires, or the like. The electronics of the IC
chip 710 may be fabricated on a silicon substrate using standard CMOS microfabrication techniques.
In this embodiment, the IC chip 710 may contain electronics for individually controlling and driving the active elements 610a and 610b of the array. For example, the electronics of the IC chip 710 may comprise multiplexers and switches for selectively coupling a signal to one of the active elements. This advantageously reduces the number of signals that need to be transmitted over a cable to and from a remote ultrasound system. The unidirectional conduction of the metal posts 633b and 633a allow the IC chip to individually address the active elements 61 Ob and 61 Oa, respectively.
Instead of bonding the IC chip to the transducer array, the IC chip may be located near the transducer array and connected to the transducer array, e.g., by wires. For example, the IC chip and transducer array may be mounted in the same housing next to each other. The IC chip may also be electrically connected to the transducer array through metal posts embedded in the matching layer as an alternative or in addition to the backing layer. Further, the electronics of the IC chip may include filters and processors for filtering and processing signals from the transducer array before sending the signals over a cable to the remote ultrasound system.
Although metal posts were used in the preferred embodiment to provide conduction through the passive layer, other conductive materials may be used for the posts.

In the foregoing specification, the invention has been described with reference to specific embodiments thereof. It will, however, be evident that various modifications and changes may be made thereto without departing from the broader spirit and scope of the invention. For example, the reader is to understand that the specific ordering and combination of process actions described herein is merely illustrative, and the invention can be performed using different or additional process actions, or a different combination or ordering of process actions. As a further example, each feature of one embodiment can be mixed and matched with other features shown in other embodiments. Additionally and obviously, features may be added or subtracted as desired. Accordingly, the invention is not to be restricted except in light of the attached claims and their equivalents.

Claims (25)

1. An ultrasound transducer comprising:
an active acoustic element; and a passive layer attached to the active acoustic element, the passive layer comprising:
a layer of material; and a plurality of conductors embedded in the layer of material.
2. The transducer of claim 1, wherein the active acoustic element comprises a piezoelectric element.
3. The transducer of claim 1, wherein the material comprises a polymer.
4. The transducer of claim 1, wherein the conductors comprise conductive posts.
5. The transducer of claim 4, wherein the plurality of conductive posts are orientated substantially perpendicular to an acoustic emitting face of the active acoustic element.
6. The transducer of claim 4, wherein the conductive posts comprise metal posts.
7. The transducer of claim 4, wherein at least one of the conductive posts extends across a thickness of the passive layer.
8. The transducer of claim 1, wherein the passive layer forms a matching layer that acoustically couples ultrasound energy from the active acoustic element or forms a backing layer that attenuates ultrasound energy propagation below the active acoustic element.
9. The transducer of claim 1, wherein at least one of the conductors extends across a thickness of the passive layer.
10. The transducer of claim 1, further comprising an electrode deposited on a surface of the passive layer, wherein the electrode is electrically coupled to the active acoustic element by at least one of the conductors.
11. An ultrasound transducer array comprising:
a plurality of active acoustic elements; and a passive layer attached to the plurality of active acoustic elements, the passive layer comprising:
a layer of material; and a plurality of conductors embedded in the layer of material.
12. The transducer array of claim 11, wherein the active acoustic element comprises a piezoelectric element.
13. The transducer array of claim 11, wherein the material comprises a polymer.
14. The transducer array of claim 11, wherein the conductors comprise conductive posts.
15. The transducer array of claim 14, wherein the plurality of conductive posts are orientated substantially perpendicular to an acoustic emitting face of the active acoustic element.
16. The transducer array of claim 14, wherein the conductive posts comprise metal posts.
17. The transducer array of claim 14, wherein at least one of the conductive posts extends across a thickness of the passive layer.
18. The transducer array of claim 11, wherein the passive layer forms a backing layer that attenuates ultrasound energy propagation below the active acoustic elements or forms a matching layer that acoustically couples ultrasound energy from the active acoustic elements.
19. The transducer array of claim 11, further comprising a plurality of electrodes deposited on a surface of the passive layer, wherein each of the electrodes is electrically coupled to one of the active acoustic elements by at least one of the conductors.
20. The transducer array of claim 19, wherein each of the electrodes is electrically coupled to a different one of the active acoustic elements.
21. The transducer array of claim 11, further comprising an integrated circuit (IC) chip electrically coupled to at least one of the active acoustic elements by at least one of the conductors.
22. The transducer array of claim 21, wherein the IC chip is bonded to the passive layer.
23. The transducer array of claim 21, wherein the IC chip comprises a plurality of electrical contacts, and each one of the electrical contacts is electrical coupled to a different one of the active acoustic elements in the transducer array by at least one of the conductors.
24. A method of fabricating a transducer, comprising:
coating a photoresist layer on an active acoustic element;
exposing the photoresist layer to light through a mask to transfer a pattern from the mask to the photoresist layer;
removing portions of the photoresist layer based on the transferred pattern to create a plurality of voids in the photoresist layer; and depositing conductive material in the voids to form conductive posts embedded in the photoresist layer.
25. The method of claim 23, further comprising curing the photoresist layer after the conductive posts are formed.
CA2709402A 2007-12-18 2008-12-15 Composite passive materials for ultrasound transducers Abandoned CA2709402A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US11/959,104 2007-12-18
US11/959,104 US7804228B2 (en) 2007-12-18 2007-12-18 Composite passive materials for ultrasound transducers
PCT/US2008/086853 WO2009079467A2 (en) 2007-12-18 2008-12-15 Composite passive materials for ultrasound transducers

Publications (1)

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CA2709402A1 true CA2709402A1 (en) 2009-06-25

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EP (1) EP2232481B1 (en)
JP (1) JP5373815B2 (en)
CA (1) CA2709402A1 (en)
WO (1) WO2009079467A2 (en)

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EP2232481B1 (en) 2019-01-23
US20100325855A1 (en) 2010-12-30
WO2009079467A2 (en) 2009-06-25
US20090156939A1 (en) 2009-06-18
JP5373815B2 (en) 2013-12-18
EP2232481A2 (en) 2010-09-29
WO2009079467A3 (en) 2010-04-22
US7804228B2 (en) 2010-09-28

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