WO2014135749A1 - Superconducting thermal detector (bolometer) of terahertz (sub-millimeter wave) radiation - Google Patents

Superconducting thermal detector (bolometer) of terahertz (sub-millimeter wave) radiation Download PDF

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WO2014135749A1
WO2014135749A1 PCT/FI2014/050158 FI2014050158W WO2014135749A1 WO 2014135749 A1 WO2014135749 A1 WO 2014135749A1 FI 2014050158 W FI2014050158 W FI 2014050158W WO 2014135749 A1 WO2014135749 A1 WO 2014135749A1
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Prior art keywords
superconducting
accordance
bolometer
layer
thermal detector
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PCT/FI2014/050158
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French (fr)
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Andrey Timofeev
Juha Hassel
Arttu Luukanen
Panu Helistö
Leif GRÖNBERG
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Teknologian Tutkimuskeskus Vtt
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Priority to US14/773,359 priority Critical patent/US10145743B2/en
Priority to EP14719807.1A priority patent/EP2965054B1/en
Publication of WO2014135749A1 publication Critical patent/WO2014135749A1/en

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00—Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J5/10—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors
    • G01J5/20—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors using resistors, thermistors or semiconductors sensitive to radiation, e.g. photoconductive devices
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00—Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J5/02—Constructional details
    • G01J5/0225—Shape of the cavity itself or of elements contained in or suspended over the cavity
    • G01J5/024—Special manufacturing steps or sacrificial layers or layer structures
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N15/00—Thermoelectric devices without a junction of dissimilar materials; Thermomagnetic devices, e.g. using the Nernst-Ettingshausen effect
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00—Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J5/10—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors
    • G01J2005/106—Arrays
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00—Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J5/10—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors
    • G01J5/20—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors using resistors, thermistors or semiconductors sensitive to radiation, e.g. photoconductive devices
    • G01J2005/208—Radiation pyrometry, e.g. infrared or optical thermometry using electric radiation detectors using resistors, thermistors or semiconductors sensitive to radiation, e.g. photoconductive devices superconductive

Definitions

  • the present invention relates to a superconducting therma l detector accordi ng to the prea m ble of Claim 1.
  • the invention a lso relates to a ma nufacturing method.
  • the invention relates also to design, fabrication, readout techniques of a superconducting thermal detector and design and methods of microwave multiplexed read-out of the arrays of superconducting thermal detectors.
  • the present invention relates also to a detector which detects electromagnetic waves at Terahertz (THz) frequencies, and more particularly to a superconducting bolometer type Terahertz wave detector.
  • THz Terahertz
  • Thermal detectors have been first introduced by S. P. Langley back in 1880.
  • the operating principle of the bolometer is based on detection a small temperature change with a sensitive thermometer, whereby the said temperature change is caused due to a heat into which the absorbed radiation is transformed in the bolometer absorbing element (Fig. 1).
  • the thermometer is isolated from the thermal reservoir through a thermal link with a thermal conductance G.
  • Thermal detectors with superconducting materials transition edge sensors (TES's)
  • TES's transition edge sensors
  • ⁇ ⁇ is a recombination time for quasiparticles.
  • the performance of non-equilibrium KID is limited by generation-recombination noise with frequency ⁇ dependent spectrum [P.K. Day , R. Barends (Ref. 5)]
  • the generation-recombination noise-limited noise equivalent power of non-equilibrium KID can be written as [Karasik 2002. Day, Barends] where mean square of the incident optical power (Popt 2 ) (1 + ( ⁇ ⁇ ) 2 )£ ⁇
  • the demonstrated by P.K. Day et al KID detector represents a superconducting quarter- wavelength transmission line resonator made out of 220 nm thick aluminium film.
  • the readout method of KID is based on microwave measurement of the complex impedance of a thin superconducting film, its equivalent circuit represents a LC resonant circuit which is capacitiveiy coupled to a transmission line.
  • the resonant circuit consists of a capacitance and an alternated by the incident radiation inductance.
  • the microwave current distribution is nonuniform in a KID device: it is mainly sensitive to the photon absorption in the centre of a superconducting strip, with maximal optical response at the shorted end of the quarter- wavelength resonator (and having zero response at the coupling end) [P.K. Day],
  • the optical absorber has to be coupled to the resonator's shorted end.
  • resonator-bolometer is an interesting option when quasiparticle recombination is too rapid, e.g., at higher temperatures, in addition the thermally suspended island provides an opportunity to spread the absorbed photon energy uniformly across the inductor, which maximizes responsivity.
  • the quasiparticle noise may be greatly reduced.
  • the noise performance of available transistor amplifiers is considerably better than is needed to reach the fundamental sensitivity limits for bolometers (e.g., photon or phonon noise ⁇ ,"
  • Imaging in the submillimetre-wave to THz spectral regions of the electromagnetic spectrum has attracted a lot of interest for various applications, in astronomical applications, cameras operating in this wavelength range can be used for mapping the Cosmic Microwave Background, interstellar gas clouds, protoplanetary disks; For Earth observation, imagery in the spectral range can be used for accurate mapping of atmospheric water vapour which is of great relevance to e.g. the greenhouse effect and also cloud formation, rainfall prediction and agriculture. In terrestrial applications the most notable so far has been the imaging of concealed items under clothing, for instance hidden weapons, explosives, drugs and other contraband.
  • Planck black body emission formula indicates the signal power at 94 GHz corresponding to a 1 K level of sensitivity at an ambient temperature of 300 K is ⁇ 260 fW (in single mode. 20 % relative bandwidth). Compare this with the single-mode power available in the LWIR (8 - 12 jim) of ⁇ 30 pW, i.e. some 2 orders of magnitude more signal power is present in the thermal infrared.
  • Another push present both in passive and active systems is the desire to operate at higher frequencies: The angular resolution of an imaging system in proportional to the ratio of the operating wavelength to the diameter of the aperture, /D, P .
  • the primary detector architectures employed at present for terrestrial passive THz imaging are a) Heterodyne down conversion receivers, b) pre-amplified direct detection receivers, or c) un- amplified direct detection receivers.
  • a ⁇ and c) can in principle operate up to several THz, whilst b) is limited by the poor availability of Low Noise Amplifiers (L As) above 300 GHz. Cost is a major issue for a) and b), while c) can be cheaper it tends to lag behind in sensitivity (at least if operated at room temperature).
  • Recent developments are focused on pushing the LNA technology deep into the submm-wave range, but it may take some time before novel submmw LNAs become affordable.
  • cryogenic passive THz video-rate imager is the system demonstrator developed by VTT in 2010-2012.
  • the system employs a linear array (128) of cryogenic antenna- coupled hot-spot microboiometers, each one of which is connected to a dedicated feedback preamplifier circuit.
  • a 2D image is formed through the use of a conical scanning optical element which essentially causes the projection of each detector at the target plane to rotate a circle.
  • a linear array of 128 detectors then draw 128 circles each slightly offset from each other in the vertical dimension.
  • An image is generated through a software routine which interpolates the data points from the scan space to Cartesian space.
  • the total parasitic conductive heat load to a 2D array with N DET detectors is N DET /2 L Q (T£— 7 ' c 2 )/i?, which is typically much more than the cooling overhead supplied by the cryocoo!er.
  • the invention is intended to eliminate the defects of the prior art described above and for this purpose create an entirely new type of superconducting thermal detector.
  • the object of the invention is a detector and readout method which allows for the construction of large format FPAs for the THz range that operate at temperatures that are readily accessible with 2-stage closed cycle cryocooiers. Similar detector arrays have been constructed for deep-cryogenic operation (T ⁇ 300 m ) (N IKA [8], MAKO [8], US!CA [10], [11]) for astrophysical applications, but due to the prohibitive cost and complexity of the associated cryogenics such systems are unusable for most terrestrial (security) applications.
  • the invention is based on a superconducting thermal detector (bolometer) where the thermometry is carried out by sensing the change in the amplitude or phase of a resonator circuit, consisting of a capacitor and a superconducting inductor where the said inductor is thermally isolated from the heat bath of the system (from the chip substrate).
  • a superconducting thermal detector bolometer
  • the senor according to the invention is characterized by what is stated in the characterizing portions of Claim 1.
  • the microfabrication method according to the invention is, in turn, characterized by what is stated in the characterizing portion of Claim 11.
  • the superconducting thermal detector (bolometer) in accordance with the invention operates in a temperature range from 1 Kelvin to 10 Kelvin ena bling much cheaper infrastructure than the deep-cryogenic devices.
  • the performance of the present invention is superior to the passive (non-cryogenic) THz detectors.
  • This invention provides a superconducting thermal detector (bolometer) to detect THz (0.1-1 THz bandwidth) radiation.
  • the temperature sensitive superconducting meander is thermally isolated from the thermal bath by micro-suspensions.
  • superconducting THz superconducting thermal detector (bolometer) and arrays of these detectors are to be used as THz radiation sensing elements (detectors) in cryogenic THz radiation passive cameras operating in two-stage cryocooiing systems.
  • Technical Descriptlori of Sypercosiductisig Thermal Detector fbobmeter in accordance with the ifwerstiori
  • the detector and readout system are based on a fundamental property of superconductors: kinetic inductance. Arising from the inertia of the superconducting charge carriers (Cooper pairs), superconductors exhibit inductance in excess of the geometric inductance associated with normal metals. Also normal metals do exhibit kinetic inductance, but the wavelengths where kinetic inductance in normal metals becomes relevant lies in the I R and optical wavelengths, whereas in superconductors the relevant frequency scale is in the THz region.
  • kinetic inductance Arising from the inertia of the superconducting charge carriers (Cooper pairs), superconductors exhibit inductance in excess of the geometric inductance associated with normal metals. Also normal metals do exhibit kinetic inductance, but the wavelengths where kinetic inductance in normal metals becomes relevant lies in the I R and optical wavelengths, whereas in superconductors the relevant frequency scale is in the THz region.
  • a kinetic inductor can be used as a thermometer to sense its physical temperature. The temperature dependent kinetic inductance is associated with the excess quasiparticle density present within the superconductor.
  • the excess quasiparticles can be generated by either incident photons (with energy greater than twice the superconducting energy gap) or through thermal excitation.
  • the phenomenon is commonly referred to as “non-equilibrium kinetic inductance”
  • the latter is “equilibrium kinetic inductance”.
  • the superconducting thermal detector is thermaily isolated from the bath enabling its efficient operation in an equilibrium regime, meaning that the incident THz radiation is absorbed by the electrons of a superconductor which are in a thermal equilibrium with its phonons at temperature T.
  • Typical temperature operation regime of such a detector lies between ⁇ Q,3T C and T c .
  • the number of quasiparticies N qp in a superconductor with a total number of electrons N depends on temperature (T ⁇ T C ) according to a two-fluid model as:
  • phonon noise greatly dominates over generation-recombination noise.
  • NEP contribution of the thermal noise due to the losses in the superconductor is few orders of magnitude lower than NEP ph .
  • a superconducting thermal detector operates in the phonon noise limit.
  • the noise equivalent power background-limited performance NEP BUP for the detector at 350 GHz is about ⁇ 1G " 1 - 5 W/Hz"' 2 for a single mode assuming quantum efficiency of unity for the 300 K black-body object emitting radiation in a 100 GHz bandwidth.
  • the NEP contributions with dissipative readout for a superconducting thermal detector (bolometer) are plotted in FIG. 4 with detector parameters as explained in the description of FIG. 4.
  • the superconducting meander line with temperature dependent inductance Li is connected to the shunting capacitor C sh to form a resonant tank circuit, which is in turn coupled to the read- out superconducting transmission line through the coupling capacitor C c (Fig. 3).
  • the detector responsivity then yields dV/dP -- ⁇ 0 5 V/W.
  • a low noise amplifier is used to readout bolometer signal.
  • the multiplexed arrays of superconducting thermal detectors represent a 2D matrix of resonant tank circuits (pixels) with alternated values of shunting capacitances in each of the resonant tank circuit (in each pixel), so that each resonant frequency is in one-to- one correspondence to a single pixel.
  • the pixels are capacitive!y coupled to a superconducting transmission line for a multiplexed microwave readout of a 2D bolometer pixel array.
  • the optimal geometry design of the said bolometer arrays is implemented to eliminate electrical cross-talk between the pixels. Proof-of-Prii ipie Validation As shown in FiG. 2A - 2B a superconducting thermal detector (bolometer) comprises the micro- structure consisting of the following parts:
  • An absorption part consisting of a resistive film 1 which absorbs THz radiation.
  • a temperature detecting part consisting of a superconducting thin film forming the inductor 2.
  • a resonant circuit consisting of the inductor 2 formed by the said superconducting film and a shunting thin film capacitor Csh, coupled to a superconducting transmission line.
  • the superconducting thermal detectors (bolometers) and arrays of those have been successfully fabricated and tested.
  • Figure 1 shows a general principle scheme of THz radiation detection with a superconducting thermal detector using the inductance in accordance with the invention.
  • Figures 2A - 2B show a schematic cross-section of thin film multi-layered structure of a superconducting thermal detector (bolometer) in accordance with the invention.
  • Figure 3 shows an equivalent electrical circuit of an array of N superconducting thermal detectors (bolometers) capacitively coupled to a superconducting transmission line in accordance with the invention.
  • Figure 6 shows a graph of measured temperature dependence of the lowest frequency resonance in the 8-pixei array of superconducting thermal detectors (bolometers) in accordance with the invention.
  • Figure 7 shows a graph of deduced from data in FIG. 6 temperature dependence of magnetic penetration length of the superconducting inductor of the superconducting thermal detector (bolometer) in accordance with the invention.
  • Figure 1 shows general principle scheme of THz radiation detection with a superconducting thermal detector using the superconducting inductance.
  • the incoming radiation is absorbed by the absorbing element 1 which is in a tight thermal contact with a superconducting inductor 2.
  • the superconducting inductor is thermally isolated from the thermal bath (substrate) by micro- suspension legs, whose total thermal conductance is denoted by G, The signal is detected by the read-out circuit 4.
  • Figure 2A shows a schematic cross-section of multi-layer structure of a superconducting thermal detector (bolometer).
  • the detector is micro-machined using standard thin film deposition and micro-lithography methods.
  • the substrate 3 represents a silicon wafer.
  • Deposited thin films on top of the silicon substrate are: 1 st layer is a silicon etch-stop layer (optional in the process), 2 na layer is a membrane layer 5, 3 rd layer is a superconducting inductor layer 2 and l 5t , t! ! layer is an insulating layer (dielectric) 7, 5 th layer is a superconducting layer 8 (optional in the process).
  • FIG. 1 shows the superconducting thermal detector (bolometer) as in FIG. 1 with an etched resonant optical 1/4 cavity 9 and a back reflector 10 to enhance optical absorptivity.
  • FIG 3 shows an equivalent electrical circuit of an array of !M superconducting thermal detectors (bolometers) capacitively coupled to a superconducting transmission line.
  • Each pixel represents an inductance Li(T) embedded into a resonant circuit with the shunting capacitor Csh J, where "i" denotes the number of the i th bolometer pixel.
  • the microwave losses of each inductor are depicted with resistor R.
  • NEP of phonon noise solid line ⁇ , thermal noise (circles), generation- recombination noise (triangles), and the background limited noise level of a blackbody with temperature 300 K in an optical bandwidth 100 GHz (dash-dotted line).
  • the quality factor of the resonators is about 300.
  • Figure 6 shows measured temperature dependence of the lowest frequency resonance in the 8-pixel array of superconducting thermal detectors (bolometers).
  • Figure 7 shows deduced from data in FIG. 5 temperature dependence of magnetic penetration length of the superconducting inductor of the superconducting thermal detector (bolometer).
  • a superconducting thermal detector of the present invention is explained with reference to FIG. 2A -- 2B with the same reference numerals as earlier.
  • the typical manufacturing process of a superconducting thermal detector includes the following micro-fabrication steps of thin film depositions and microlithography patterning methods: 1. Deposition of etch-stop layer such as silicon oxide or onto a silicon substrate 3
  • the membrane layer comprises a 100 nm to 1 ⁇ thick film of a material such as a silicon nitride (SiN, 5i 3 ), a silicon oxide (SiO, Si0 2 ), or other-like materials used to form membranes.
  • a material such as a silicon nitride (SiN, 5i 3 ), a silicon oxide (SiO, Si0 2 ), or other-like materials used to form membranes.
  • the superconducting inductor comprises a 3 nm to 500 nm thick film of a superconducting material such as niobium (Nb), niobium nitride (NbN) or niobium titanium nitride (NbTiN).
  • a superconducting material such as niobium (Nb), niobium nitride (NbN) or niobium titanium nitride (NbTiN).
  • the material of superconducting inductor layer 6 is not limited to Nb, NbN, or NbTiN, and other superconducting materials such as aluminium (Al), vanadium (V), vanadium nitride (VIM), tungsten siiicide (WSi), magnesium diboride (MgB 2 ) and other-like can be used.
  • the superconducting inductor layer 6 is patterned by micro-lithography and by wet etching or by plasma etching.
  • the insulator layer 7 material comprises a 10 nm to 1 ⁇ thick film of silicon nitride (SiN, Si 3 N ), a silicon oxide (SiO, Si0 2 ), aluminium oxide (AIO, Al 2 0 3 ), or other-like insulator materials.
  • the insulator layer 7 is patterned by micro-lithography and by wet etching or by plasma etching.
  • 2 nd superconducting layer 8 comprising a 3 nm to 1 ⁇ thick film comprising any of superconducting materials listed in the step 3 of deposition of superconducting inductor layer 6.
  • the 2 nd superconducting layer 8 is patterned by micro-lithography and by wet etching or by plasma etching.
  • absorbing element 1 comprises a normal metal 100 nm thick film of titanium tungsten (TiW).
  • TiW titanium tungsten
  • the material of absorbing element 1 is not limited to TiW, and other metallic materials such as Mo, Ti and the like can be used to form the absorbing element 1.
  • Optional step Forming membrane perforations 21 and micro-suspension legs 11 to enhance thermal isolation of a superconducting inductor 2 or/and absorbing element 1.
  • the perforations 21 in the membrane layer 5 are patterned by micro-lithography and by wet etching or by plasma etching.
  • an optical cavity 9 of a gap of A/4 or odd multiples of A/4: (2n + 1)1/4, (n 1,2, . . . ) can be formed between an absorbing element 1 and the attached back reflector 10.
  • A/4 ⁇ 214 ⁇ or 3 ⁇ /4— 643 ⁇ or optical cavity the wavelength A ⁇ 857 ⁇ for incoming 350 GHz radiation
  • the silicon wafer substrates 3 with corresponding approximate thicknesses of A/4 and 3A/4 are used in the microfabrication process of a superconducting thermal detector (bolometer).
  • a back reflector 10 can comprise a reflective surface or a reflective film deposited onto another substrate, which are attached to the substrate 3. 9. (Optional step). Removing etch-stop silicon oxide layer in a buffered HF solution or in a dry HF vapour etcher.
  • thermometry is carried out by sensing the change in the amplitude or phase of a resonator circuit, consisting of a capacitor and a superconducting inductor where the said superconducting inductor is thermally isolated from the heat bath of the system.
  • a superconducting thermal detector (bolometer) described in paragraph 1) where the inductor phonon system is located on the membrane thermally isolated from the phonon system of the lattice by micro-suspensions.
  • a superconducting thermal detector (bolometer) of paragraph 1) wherein the said superconducting inductor comprises a superconducting material comprising nitrogen (N) and a metal selected form the group consisting of Niobium (Nb), Titanium (Ti) and Vanadium (V).
  • a superconducting thermal detector (bolometer) utilizing kinetic inductance thermometry which is read out by a scattering parameter measurement which can be used to determine the amplitude or phase change in the resonator induced by impinging optical power.
  • a superconducting thermal detector (bolometer) of paragraph 1) which utilizes kinetic inductance thermometry and incorporates an impedance matching surface for efficient absorption of incident optical power.
  • a superconducting thermal detector (bolometer) of paragraph 1) which utilizes kinetic inductance thermometry and incorporates an antenna and an antenna termination which dissipates the incident radiation power and translates it to heat to be sensed by the kinetic inductance thermometer.
  • the read-out circuit of incident THz radiation signal that is implemented by sensing microwave transmission/reflection parameters via a superconducting transmission line to which the said superconducting thermal detector (bolometer) of any of paragraphs 1) to 7) is coupled either via a capacitance or via an inductance or via a circuit containing both an inductance and a capacitance.
  • the bolometer array circuit comprising linear or 2-dimensional matrix of superconducting thermal defectors
  • bolometers consists of individual bolometer resonant circuits with different resonant frequencies coupled to a superconducting transmission line via a capacitance or via an inductance or via a circuit containing both inductive and a capacitive elements.
  • IVIAKQ a pathfinder instrument for on-sky demonstration of k

Abstract

A superconducting thermal detector (bolometer) of THz (sub-millimeter) wave radiation based on sensing the change in the amplitude or phase of a resonator circuit, consisting of a capacitor (Csh) and a superconducting temperature dependent inductor (2) where the said inductor is thermally isolated from the heat bath (chip substrate (3)) by micro-suspensions (11). The bolometer design includes a thin film inductor located on the membrane, a single or/and multi-layered thin film capacitor, and a thin film absorber of incoming radiation. The bolometer design can also include a lithographic antenna with antenna termination and/or a back reflector beneath the membrane for optimal wavelength detection by the resonance circuit. The superconducting thermal detector (bolometer) and arrays of these detectors operate in a temperature range from 1 Kelvin to 10 Kelvin.

Description

U PERCONDUCT!NG TH ERMAL DETECTOR f BOLOMETER) OF TERAH E
! LUM ETER WAVE) R DEON
FIELD OF THE INVEMTI!ON
The present invention relates to a superconducting therma l detector accordi ng to the prea m ble of Claim 1.
The invention a lso relates to a ma nufacturing method.
The invention relates also to design, fabrication, readout techniques of a superconducting thermal detector and design and methods of microwave multiplexed read-out of the arrays of superconducting thermal detectors.
The present invention relates also to a detector which detects electromagnetic waves at Terahertz (THz) frequencies, and more particularly to a superconducting bolometer type Terahertz wave detector.
BACKGROUND OF THE INVENTION
Thermal detectors (bolometers) have been first introduced by S. P. Langley back in 1880. The operating principle of the bolometer is based on detection a small temperature change with a sensitive thermometer, whereby the said temperature change is caused due to a heat into which the absorbed radiation is transformed in the bolometer absorbing element (Fig. 1). For sensitivity, the thermometer is isolated from the thermal reservoir through a thermal link with a thermal conductance G. Thermal detectors with superconducting materials (transition edge sensors (TES's)) based on sharp temperature dependence of the resistance within the superconducting transition have been first proposed in late 1930's [D.H. Andrews, Yearbook - Am. Philos. Soc. (1938), 132: A. Goetz, Phys. Rev. 55, 1270, 1939] and demonstrated in early 1940's [ D. H. Andrews et a!., Phys. Rev. 59, 1045, 1941] . In late 1980's D.G. McDonald proposed [Applied Physics Letters, Vol. 50, p. 775, 1987] and demonstrated shortly after a superconducting bolometer based on kinetic inductance of a superconducting microstrip line [IEEE Trans, on Magnetics, Vol. 25, No. 2, 1989]. Its operation is based on strong temperature T dependence of the kinetic inductance near the transition temperature T of a superconductor (T < Tc .
RELATED PATENT DOCUMENT
Also known in the prior art is Donald G. McDonald, U.S. Patent No. 4,869,598, issued Sep. 26 1989 (which has an expired status at 2012), which is said (in its claim 1) to disclose a temperature-sensitive superconducting device comprising a sensor having a geometry with at least two operationally interacting spaced superconducting thin film layers separated by dielectric, wherein the said sensor has a temperature dependent kinetic inductance based upon a magnetic penetration depth. Among the number of disclosed devices based on the said sensor in this invention (in the claims from 1 to 25), it is said to disclose the device based on utilizing said sensor to receive said temperature indicative output (claim 7); the device utilizing said sensor used as a variable inductance for electronic circuit means (claim 13); the device with electronic circuit means including oscillation means providing an output frequency varying due to temperature dependent inductance, whereby the output frequency of said oscillations means is temperature dependent (claim 14); the device of claim 1 including means for connecting said sensor with monitoring means capable of monitoring at least one of power and radiation whereby said device produces a temperature-indicative output that is indicative of at least one of power and radiation monitored by said monitor means (claim 15); superconductor-based detection devices comprising absorbing elements of at least one of power and radiation (claims 19 - 25). FURTHER PRIOR ART
FIRST IMPLEME TATION OF FAR-SNFRARED (THZ) KI ETIC INDUCTA CE BOLOMETERS
The first demonstration of kinetic inductance bolometers with coupled antenna absorber by using SQUID read-out scheme was carried out in 1991 by E.N. Grossman, D.G. McDonald and J. E. Saifvageau [see IEEE Trans. On Magnetics. Vol. 27, No. 2, March 1991, 2677-2680; 2757- 2760].
MULTIPLEXABLE MICROWAVE KINET!C [INDUCTANCE THZ DETECTORS Recently introduced microwave kinetic inductance detectors opened possibility to build multi- pixel superconducting THz imaging arrays with hundreds of pixel readout out only with a single pair of coaxial lines. Below in the text we give a brief overview of these detectors.
KID
in 2003 P. K. Day et al [Nature, Vol. 425, p. 817, 2003, (Ref. 4)] demonstrated kinetic inductance detector (KID) operating in non-equilibrium mode at temperatures T much below the transition temperature Tc (T « Tc), The microscopic physical mechanism of KID operation is based on breaking Cooper pairs into quasiparticles in a superconductor by incident photons with energies larger than twice of a superconducting gap. As a consequence, the kinetic inductance of a superconductor changes proportionally to the change of quasiparficle density caused by incident radiation. For KID, the change of kinetic inductance under irradiated optical power Popt can be written as d k dl-k ¾n
dPopt "" dNqp dPopt where Nqp is a number of quasiparticles in a superconductor, where the incident optical power converted with optical efficiency η into quasiparticles in a steady state is Popt =
Figure imgf000004_0001
Here ττ is a recombination time for quasiparticles. The performance of non-equilibrium KID is limited by generation-recombination noise with frequency ω dependent spectrum [P.K. Day , R. Barends (Ref. 5)]
5 (ω) = Γ„ (1),
The generation-recombination noise-limited noise equivalent power of non-equilibrium KID can be written as [Karasik 2002. Day, Barends]
Figure imgf000004_0002
where mean square of the incident optical power (Popt2) (1 + (ωτΓ)2)£ίω
Figure imgf000005_0001
is expressed through the generation-recombination noise spectrum SN of the quasiparticles in a superconductor with the response time τΓ.
The demonstrated by P.K. Day et al KID detector represents a superconducting quarter- wavelength transmission line resonator made out of 220 nm thick aluminium film. The readout method of KID is based on microwave measurement of the complex impedance of a thin superconducting film, its equivalent circuit represents a LC resonant circuit which is capacitiveiy coupled to a transmission line. The resonant circuit consists of a capacitance and an alternated by the incident radiation inductance. The microwave current distribution is nonuniform in a KID device: it is mainly sensitive to the photon absorption in the centre of a superconducting strip, with maximal optical response at the shorted end of the quarter- wavelength resonator (and having zero response at the coupling end) [P.K. Day], Thus, in the said KID device the optical absorber has to be coupled to the resonator's shorted end.
LEK!D
As a modification of KID, in 2007 S. Doyle demonstrated lumped element kinetic inductance detector (LEKID) device [S. Doyle et al, 32nd International Conference on Infrared and Millimeter Waves IRMMW-THz, pp. 450-451, 2007], in which the capacitance of the resonant circuit is formed by interdigital capacitor fingers. This geometrical configuration provides a uniform microwave current distribution in the resonator and the resonator itself acts both as an optical absorber and as a sensing element. The equivalent electrical circuit of LEKID device represents a series superconducting LC circuit inductively coupled to a read-out superconducting transmission line.
SUPERCONDUCTING MICRORESONA TOR BOLOMETERS it has been also pointed out by Jonas Zmuidzinas in 2012 [Annu, Rev. Condens. Matter Phys. 2012. 3:169-214] that [citation taken from the text]: "Superconducting microresonators have been successfully fabricated on thermally suspended silicon nitride micromesh [personal communications with H.G, Leduc and P.K. Day, 2010], so a frequency-multiplexed array of bolometers is straightforward to produce. In a standard MKiD, quasiparticle recombination provides the bottleneck for power flow, whereas in a bolometer, the bottleneck [for power flow] is set by the geometry of the thermal suspension legs. Therefore, resonator-bolometer is an interesting option when quasiparticle recombination is too rapid, e.g., at higher temperatures, in addition the thermally suspended island provides an opportunity to spread the absorbed photon energy uniformly across the inductor, which maximizes responsivity. In addition, the quasiparticle noise may be greatly reduced. Finally, the noise performance of available transistor amplifiers is considerably better than is needed to reach the fundamental sensitivity limits for bolometers (e.g., photon or phonon noise},"
Below, in chapter "Technical Description of Superconducting thermal detector (bolometer)", we present detailed theory and experimental data for fabricated arrays of superconducting thermal detectors (bolometers). TERAHERTZ ifVl G!MG
Imaging in the submillimetre-wave to THz spectral regions of the electromagnetic spectrum has attracted a lot of interest for various applications, in astronomical applications, cameras operating in this wavelength range can be used for mapping the Cosmic Microwave Background, interstellar gas clouds, protoplanetary disks; For Earth observation, imagery in the spectral range can be used for accurate mapping of atmospheric water vapour which is of great relevance to e.g. the greenhouse effect and also cloud formation, rainfall prediction and agriculture. In terrestrial applications the most notable so far has been the imaging of concealed items under clothing, for instance hidden weapons, explosives, drugs and other contraband. This application benefits from i) the relative good penetration of the radiation in the said wavelength range and 11} the wavelengths in general which are short enough that image forming instruments can be developed which possess an aperture diameter less than one meter. OVERVIEW OF PASSIVE THZ !!V!AGS G TECHNOLOGY
Passive imaging poses challenges with respect to the receiver sensitivity, given the weakness of the (thermal) signatures. For passive systems the Planck black body emission formula indicates the signal power at 94 GHz corresponding to a 1 K level of sensitivity at an ambient temperature of 300 K is ~ 260 fW (in single mode. 20 % relative bandwidth). Compare this with the single-mode power available in the LWIR (8 - 12 jim) of ~30 pW, i.e. some 2 orders of magnitude more signal power is present in the thermal infrared. Another push present both in passive and active systems is the desire to operate at higher frequencies: The angular resolution of an imaging system in proportional to the ratio of the operating wavelength to the diameter of the aperture, /D,P. Given that end-users typically want to minimize the aperture size (and the system volume), operation at higher frequencies facilitates better angular resolution. In addition, many imaging applications including security, requires relatively large Field-of-View (FoV). Covering a large FoV with good angular resolution requires either large number of receivers (hundreds to thousands), or the combination of scanning with a smaller FPA. Due to cost, latter is often unavoidable.
The primary detector architectures employed at present for terrestrial passive THz imaging are a) Heterodyne down conversion receivers, b) pre-amplified direct detection receivers, or c) un- amplified direct detection receivers. Of these a} and c) can in principle operate up to several THz, whilst b) is limited by the poor availability of Low Noise Amplifiers (L As) above 300 GHz. Cost is a major issue for a) and b), while c) can be cheaper it tends to lag behind in sensitivity (at least if operated at room temperature). Recent developments are focused on pushing the LNA technology deep into the submm-wave range, but it may take some time before novel submmw LNAs become affordable. Packaging and assembly of M IC's plays a major role here, not to mention device testing costs. in passive imaging mode, the simultaneous requirements for sensitivity, large pixel count, large FoV and operation in the submm-wave range has motivated the development of cryogenic imaging systems. With cooling it is possible to substantially increase the sensitivity of bolometers to the point where they outperform any room temperature (even pre-amplified) detector technology. While the introduction of a closed-cycle cooling adds cost, weight, power draw and footprint to the camera back-end, the front-end is in fact less complicated than with e.g. heterodyne or preamp!ified direct detection architectures. Cooled systems also can leverage from the rapid development of compact cryocoolers which are now in widespread use in medical MR I machines.
An example of a cryogenic passive THz video-rate imager is the system demonstrator developed by VTT in 2010-2012. The system employs a linear array (128) of cryogenic antenna- coupled hot-spot microboiometers, each one of which is connected to a dedicated feedback preamplifier circuit. A 2D image is formed through the use of a conical scanning optical element which essentially causes the projection of each detector at the target plane to rotate a circle. A linear array of 128 detectors then draw 128 circles each slightly offset from each other in the vertical dimension. An image is generated through a software routine which interpolates the data points from the scan space to Cartesian space.
Whilst this approach can he used to build a camera as has successfully been demonstrated the approach suffers from several shortcomings: i) A linear array necessitates a (large) optomechanical scanner which increases system complexity and rises maintenance and reliability issues, ii) the dynamic range of the image is reduced due to the short dwell time per image pixel, increasing the noise bandwidth (while the information bandwidth is not increased).
Passive THz smagmg focal arses A passive imager would greatly benefit from a 2D focal plane array (FPA): in order to generate an image with Nip image pixels with Ndet detectors (Nip > Ndet), there has to be n = NJP/NDE† scan positions for each frame. An application typically dictates a required frame-rate [frame - Thus the per-pixei integration time is given by £int = l/(n f fr me) ~^ιε signal-to-noise ratio of a detector is proportional to ^jtint (assuming white noise). Thus, the less scanning is required to cover the needed image pixel count, the better the SNR will be.
Whilst large format FPAs are prevalent in spectral ranges beyond THz (!R, visible etc.), the THz range has yet to see the advent of large 2D FPAs. This is due to the aforementioned high costs of room-temperature detectors (primarily preamplified suhm n-wave direct detection receivers utilizing InP LNAs), and the unavailability of cryogenic multiplexing methods and detectors operating in the temperature range 1 K < T < 10 K. The approach detailed above (parallel readout of 128 channels) does not scale to 2D arrays if using multiplexing at room temperature: each detector element in the array requires at least 2 low-impedance signal lines from the cryogenic FPA to room temperature. The conducted thermal heat load per signal wire is approximately Qw = 1/2 ί0(τξ - T?)/R where L0 = 2.45 xlO'8 V2/K2 is the Lorentz constant, R is the average wire resistance and TH and TC are the hot and cold stage temperatures, respectively. Thus, the total parasitic conductive heat load to a 2D array with NDET detectors is NDET/2 LQ (T£— 7' c 2)/i?, which is typically much more than the cooling overhead supplied by the cryocoo!er. The invention is intended to eliminate the defects of the prior art described above and for this purpose create an entirely new type of superconducting thermal detector. The object of the invention is a detector and readout method which allows for the construction of large format FPAs for the THz range that operate at temperatures that are readily accessible with 2-stage closed cycle cryocooiers. Similar detector arrays have been constructed for deep-cryogenic operation (T < 300 m ) (N IKA [8], MAKO [8], US!CA [10], [11]) for astrophysical applications, but due to the prohibitive cost and complexity of the associated cryogenics such systems are unusable for most terrestrial (security) applications.
The invention is based on a superconducting thermal detector (bolometer) where the thermometry is carried out by sensing the change in the amplitude or phase of a resonator circuit, consisting of a capacitor and a superconducting inductor where the said inductor is thermally isolated from the heat bath of the system (from the chip substrate).
More specifically, the sensor according to the invention is characterized by what is stated in the characterizing portions of Claim 1. The microfabrication method according to the invention is, in turn, characterized by what is stated in the characterizing portion of Claim 11.
Considerable advantages are gained with the aid of the invention. The superconducting thermal detector (bolometer) in accordance with the invention operates in a temperature range from 1 Kelvin to 10 Kelvin ena bling much cheaper infrastructure than the deep-cryogenic devices. On the other hand the performance of the present invention is superior to the passive (non-cryogenic) THz detectors. SUMMARY OF THE S! EIS!TSOIS!
This invention provides a superconducting thermal detector (bolometer) to detect THz (0.1-1 THz bandwidth) radiation. In this device, the temperature sensitive superconducting meander is thermally isolated from the thermal bath by micro-suspensions. Described in this invention superconducting THz superconducting thermal detector (bolometer) and arrays of these detectors are to be used as THz radiation sensing elements (detectors) in cryogenic THz radiation passive cameras operating in two-stage cryocooiing systems. Technical Descriptlori of Sypercosiductisig Thermal Detector fbobmeter) in accordance with the ifwerstiori
Theory of operation of Superconducting Thermal Detector (bolometer) The detector and readout system are based on a fundamental property of superconductors: kinetic inductance. Arising from the inertia of the superconducting charge carriers (Cooper pairs), superconductors exhibit inductance in excess of the geometric inductance associated with normal metals. Also normal metals do exhibit kinetic inductance, but the wavelengths where kinetic inductance in normal metals becomes relevant lies in the I R and optical wavelengths, whereas in superconductors the relevant frequency scale is in the THz region.
An important feature of the kinetic inductance L¾ is that it is strongly temperature T dependent: Lk = Lfe (0)/'(1— CT/rc)4), where Tc is the transition temperature of a superconductor, Lk (Q) «
Figure imgf000010_0001
for a narrow thin superconducting strip, with magnetic penetration depth λ^ϋ), having a geometry of length I, width w and thickness d. Owing to this property, a kinetic inductor can be used as a thermometer to sense its physical temperature. The temperature dependent kinetic inductance is associated with the excess quasiparticle density present within the superconductor. The excess quasiparticles can be generated by either incident photons (with energy greater than twice the superconducting energy gap) or through thermal excitation. In the former case the phenomenon is commonly referred to as "non-equilibrium kinetic inductance", whereas the latter is "equilibrium kinetic inductance". in the present invention the superconducting thermal detector is thermaily isolated from the bath enabling its efficient operation in an equilibrium regime, meaning that the incident THz radiation is absorbed by the electrons of a superconductor which are in a thermal equilibrium with its phonons at temperature T. Typical temperature operation regime of such a detector lies between ~ Q,3TC and Tc . The number of quasiparticies Nqp in a superconductor with a total number of electrons N depends on temperature (T~TC ) according to a two-fluid model as:
Figure imgf000011_0001
For a superconducting thermal detector with kinetic inductance Lk/ which has thermal isolations (micro-suspensions) with thermal conductance G, the variations of the kinetic inductance under the incident optical power can be written as
r]G d.T assuming that the incident optical power dPopt = ηΰάΤ is absorbed with optical efficiency ?j and converted into heat. For a superconducting thermal detector with thermal response time Tthl the generation-recombination noise-limited noise equivalent power in the equilibrium case can be written then as
NEPg e5r = j(Popt 2)/d<o = JsLk (1 + («¾>)*)/ (^) =^SNqp (l + (ωτΓ)2) / , (3) where
Figure imgf000011_0002
so that using equations (1), (2), (3), and (4) from above we have
With typical numbers for G ~ 100 nW/ at T = 5 for SiN microsuspensions, τΓ < ~1 ns, Nqp ~ N 0) x EF x Vol ~ 1015 quasiparticies in the superconductor with length i~10~2 m, width ί— 10 ~ 6 m, and thickness d~ 10- 7 m, yielding the volume Vol = ivvd~ 10-15 m3, and with the values (of the order of magnitude) for the density of electron states N (Q) ~ 1047 m"3."1 and Fermi energy EF ~ 10~18 J in metals, we have for ?j < 1: NEPg1r < ~2,5 x 10" 19 W/Hz1^'. The thermal fluctuation (phonon) noise-limited noise equivalent power
NEPph = y/ kBT2 G yields NEPph < ~10- 14 W/Hz1''2 (at 7 = 5 K). Thus in the superconducting thermal detector (bolometer) phonon noise greatly dominates over generation-recombination noise. Also, with typical device parameters NEP contribution of the thermal noise due to the losses in the superconductor (finite quality factor of the resonant circuit) is few orders of magnitude lower than NEPph. Thus, a superconducting thermal detector operates in the phonon noise limit. The noise equivalent power background-limited performance NEPBUP for the detector at 350 GHz is about ~ 1G " 1-5 W/Hz"'2 for a single mode assuming quantum efficiency of unity for the 300 K black-body object emitting radiation in a 100 GHz bandwidth. The NEP contributions with dissipative readout for a superconducting thermal detector (bolometer) are plotted in FIG. 4 with detector parameters as explained in the description of FIG. 4.
For a microwave read-out of a superconducting thermal detector (bolometer), the superconducting meander line with temperature dependent inductance Li ) is connected to the shunting capacitor Csh to form a resonant tank circuit, which is in turn coupled to the read- out superconducting transmission line through the coupling capacitor Cc (Fig. 3). With typical value for thermal conductance of micro-suspensions G— 100 nW/'K and linear dimensions of a superconducting inductor said above, the detector responsivity then yields dV/dP --Ί05 V/W. A low noise amplifier is used to readout bolometer signal. The multiplexed arrays of superconducting thermal detectors (multiplexed pixels) represent a 2D matrix of resonant tank circuits (pixels) with alternated values of shunting capacitances in each of the resonant tank circuit (in each pixel), so that each resonant frequency is in one-to- one correspondence to a single pixel. The pixels are capacitive!y coupled to a superconducting transmission line for a multiplexed microwave readout of a 2D bolometer pixel array. The optimal geometry design of the said bolometer arrays is implemented to eliminate electrical cross-talk between the pixels. Proof-of-Prii ipie Validation As shown in FiG. 2A - 2B a superconducting thermal detector (bolometer) comprises the micro- structure consisting of the following parts:
1) An absorption part consisting of a resistive film 1 which absorbs THz radiation.
2} A temperature detecting part consisting of a superconducting thin film forming the inductor 2.
3} A resonant circuit consisting of the inductor 2 formed by the said superconducting film and a shunting thin film capacitor Csh, coupled to a superconducting transmission line.
4) A back reflector 10 attached at the bottom of the Si chip and forming A/4 opticai cavity 9 for enhanced THz absorption (Figure 2B).
The superconducting thermal detectors (bolometers) and arrays of those have been successfully fabricated and tested. The experimental data shown in FiG. 5 demonstrates a multiplexed 8-pixei bolometer array measured at a reduced temperature T/Tc = 0.9 with 7 ~ 4 K.
The measured temperature dependence of the resonant frequency is shown in FiG. 6. in FiG. 7 we show temperature dependence of kinetic inductance the deduced from data in FIG. 6 (circles). The solid lines are the fits according to two-fluid model Lk = Lfc(0)/(1 - (Γ/7 )4) with critical temperature Tc = 4.03 K and magnetic penetration depth A(0) = 626 nm.
DESCRIPTOR OF FIGURES
The following reference numbers will be used in connection with the following terms:
1 absorbing element
2 superconducting inductor
substrate
4 read-out circuit
5 membrane layer 6 superconducting inductor layer (1st superconducting electrode)
7 insulator layer
8 2nd superconducting layer (2nd superconducting electrode)
9 optical cavity
10 back reflector
11 micro-suspensions
21 membrane perforations
Csh shunting thin film capacitor
The features of the invention can be understood with reference to the drawings and the graphs described below, and the claims. The drawings are not necessarily to scale, emphasizing instead the principles and key features of the invention. In the drawings, numerals are used to indicate throughout the views. in the following, the invention is examined with the aid of examples and with reference to the accompanying drawings.
Figure 1 shows a general principle scheme of THz radiation detection with a superconducting thermal detector using the inductance in accordance with the invention.
Figures 2A - 2B show a schematic cross-section of thin film multi-layered structure of a superconducting thermal detector (bolometer) in accordance with the invention.
Figure 3 shows an equivalent electrical circuit of an array of N superconducting thermal detectors (bolometers) capacitively coupled to a superconducting transmission line in accordance with the invention.
Figure 4 shows a graph of calculated noise-equivalent power (NEP) contributions with optical efficiency of unitv for a superconducting thermal detector (bolometer) in accordance with the invention at reduced temperatures T/Tc = 0.3 ... 1.
Figure 5 shows a graph of measured transmission S21 parameter in decibels for 8-pixel array of superconducting thermal detectors (bolometers) in accordance with the invention at a reduced temperature T/T = 0.9. Figure 6 shows a graph of measured temperature dependence of the lowest frequency resonance in the 8-pixei array of superconducting thermal detectors (bolometers) in accordance with the invention.
Figure 7 shows a graph of deduced from data in FIG. 6 temperature dependence of magnetic penetration length of the superconducting inductor of the superconducting thermal detector (bolometer) in accordance with the invention. DETAILED DESCRIPTION OF F!GURES
Figure 1 shows general principle scheme of THz radiation detection with a superconducting thermal detector using the superconducting inductance. The incoming radiation is absorbed by the absorbing element 1 which is in a tight thermal contact with a superconducting inductor 2. The superconducting inductor is thermally isolated from the thermal bath (substrate) by micro- suspension legs, whose total thermal conductance is denoted by G, The signal is detected by the read-out circuit 4.
Figure 2A shows a schematic cross-section of multi-layer structure of a superconducting thermal detector (bolometer). The detector is micro-machined using standard thin film deposition and micro-lithography methods. The substrate 3 represents a silicon wafer. Deposited thin films on top of the silicon substrate are: 1st layer is a silicon etch-stop layer (optional in the process), 2na layer is a membrane layer 5, 3rd layer is a superconducting inductor layer 2 and l5t , t! ! layer is an insulating layer (dielectric) 7, 5th layer is a superconducting layer 8 (optional in the process). The perforations 21 (optional in the process) in the membrane layer 5 are applied to form narrow micro-suspension legs for thermal insulation. The deep silicon etch through the substrate 3 is applied to form resonant optical 1/4 cavity 9. Figure 2B shows the superconducting thermal detector (bolometer) as in FIG. 1 with an etched resonant optical 1/4 cavity 9 and a back reflector 10 to enhance optical absorptivity.
Figure 3 shows an equivalent electrical circuit of an array of !M superconducting thermal detectors (bolometers) capacitively coupled to a superconducting transmission line. Each pixel represents an inductance Li(T) embedded into a resonant circuit with the shunting capacitor Csh J, where "i" denotes the number of the ith bolometer pixel. The microwave losses of each inductor are depicted with resistor R. Figure 4 shows a calculated noise-equivalent power (NEP) contributions for a superconducting thermal detector (bolometer) at reduced temperatures T/Tc = 0.3 ... 1 assuming unity for optical efficiency: NEP of phonon noise (solid line}, thermal noise (circles), generation- recombination noise (triangles), and the background limited noise level of a blackbody with temperature 300 K in an optical bandwidth 100 GHz (dash-dotted line). The thermal conductance of micro-suspensions is assumed to be temperature dependent as G(T) = 50 nVV/K * (T/Tc 1 assuming temperature dependent lattice thermal isolation ~7'3 of an insulating material of microsuspensions [Ref. 12],
Figure 5 shows measured transmission S21 parameter in decibels for 8-pixel array of superconducting thermal detectors (bolometers) at a reduced temperature T/'TC = 0.9. The quality factor of the resonators is about 300.
Figure 6 shows measured temperature dependence of the lowest frequency resonance in the 8-pixel array of superconducting thermal detectors (bolometers).
Figure 7 shows deduced from data in FIG. 5 temperature dependence of magnetic penetration length of the superconducting inductor of the superconducting thermal detector (bolometer).
Some preferred embodiments of the invention are listed in the following paragraphs:
MA!SiUFACTUR!!SiG METHOD of Superconducting thermal detector (bo ometer) of Terahertz (sub-miHirrieter) wave radiatsors in accordance with the irswerstiors
In the following, manufacturing method of a superconducting thermal detector (bolometer) of the present invention is explained with reference to FIG. 2A -- 2B with the same reference numerals as earlier. The typical manufacturing process of a superconducting thermal detector (bolometer) includes the following micro-fabrication steps of thin film depositions and microlithography patterning methods: 1. Deposition of etch-stop layer such as silicon oxide or onto a silicon substrate 3
(optional step).
2. Deposition of the membrane layer 5 onto the silicon substrate 3. The membrane layer comprises a 100 nm to 1 μηι thick film of a material such as a silicon nitride (SiN, 5i3 ), a silicon oxide (SiO, Si02), or other-like materials used to form membranes.
3. Deposition of superconducting inductor layer 6 is done by sputtering method in argon atmosphere. The superconducting inductor comprises a 3 nm to 500 nm thick film of a superconducting material such as niobium (Nb), niobium nitride (NbN) or niobium titanium nitride (NbTiN). The material of superconducting inductor layer 6 is not limited to Nb, NbN, or NbTiN, and other superconducting materials such as aluminium (Al), vanadium (V), vanadium nitride (VIM), tungsten siiicide (WSi), magnesium diboride (MgB2) and other-like can be used. The superconducting inductor layer 6 is patterned by micro-lithography and by wet etching or by plasma etching.
4. Deposition of insulator layer 7. The insulator layer 7 material comprises a 10 nm to 1 μίϊΐ thick film of silicon nitride (SiN, Si3N ), a silicon oxide (SiO, Si02), aluminium oxide (AIO, Al203), or other-like insulator materials. The insulator layer 7 is patterned by micro-lithography and by wet etching or by plasma etching.
5. (Optional step) Deposition of 2nd superconducting layer 8 comprising a 3 nm to 1 πΊ thick film comprising any of superconducting materials listed in the step 3 of deposition of superconducting inductor layer 6. The 2nd superconducting layer 8 is patterned by micro-lithography and by wet etching or by plasma etching.
6. Deposition of absorber layer followed by wet etching or by dry etching to form absorbing element 1. The material of an absorbing element 1 comprises a normal metal 100 nm thick film of titanium tungsten (TiW). The material of absorbing element 1 is not limited to TiW, and other metallic materials such as Mo, Ti and the like can be used to form the absorbing element 1.
(Optional step). Forming membrane perforations 21 and micro-suspension legs 11 to enhance thermal isolation of a superconducting inductor 2 or/and absorbing element 1. The perforations 21 in the membrane layer 5 are patterned by micro-lithography and by wet etching or by plasma etching.
Deep etching of silicon to release the membrane layer 5 by anisotropic silicon ICP etching or by wet etching. To enhance absorption of THz radiation, an optical cavity 9 of a gap of A/4 or odd multiples of A/4: (2n + 1)1/4, (n = 1,2, . . . ) can be formed between an absorbing element 1 and the attached back reflector 10. To form A/4 ~ 214 μπι or 3Λ/4— 643 μπϊ or optical cavity (the wavelength A ~ 857 μπι for incoming 350 GHz radiation) the silicon wafer substrates 3 with corresponding approximate thicknesses of A/4 and 3A/4 are used in the microfabrication process of a superconducting thermal detector (bolometer). A back reflector 10 can comprise a reflective surface or a reflective film deposited onto another substrate, which are attached to the substrate 3. 9. (Optional step). Removing etch-stop silicon oxide layer in a buffered HF solution or in a dry HF vapour etcher.
Some preferred embodiments of the invention are listed in the following paragraphs:
A superconducting thermal detector (bolometer) where the thermometry is carried out by sensing the change in the amplitude or phase of a resonator circuit, consisting of a capacitor and a superconducting inductor where the said superconducting inductor is thermally isolated from the heat bath of the system.
A superconducting thermal detector (bolometer) described in paragraph 1) where the inductor phonon system is located on the membrane thermally isolated from the phonon system of the lattice by micro-suspensions.
A superconducting thermal detector (bolometer) of paragraph 1). wherein the said inductor comprises a superconducting material having a high normal state resistivity. 4) A superconducting thermal detector (bolometer) of paragraph 1), wherein the said superconducting inductor comprises a superconducting material such as aluminium (Al), Niobium (Nb), Vanadium (V), Tungsten silicide (WSi), Magnesium diboride ( gB2), and other-iike superconducting materials.
A superconducting thermal detector (bolometer) of paragraph 1), wherein the said superconducting inductor comprises a superconducting material comprising nitrogen (N) and a metal selected form the group consisting of Niobium (Nb), Titanium (Ti) and Vanadium (V).
5) A superconducting thermal detector (bolometer) utilizing kinetic inductance thermometry which is read out by a scattering parameter measurement which can be used to determine the amplitude or phase change in the resonator induced by impinging optical power.
6) A superconducting thermal detector (bolometer) of paragraph 1) which utilizes kinetic inductance thermometry and incorporates an impedance matching surface for efficient absorption of incident optical power.
7) A superconducting thermal detector (bolometer) of paragraph 1) which utilizes kinetic inductance thermometry and incorporates an antenna and an antenna termination which dissipates the incident radiation power and translates it to heat to be sensed by the kinetic inductance thermometer.
8) The read-out circuit of incident THz radiation signal that is implemented by sensing microwave transmission/reflection parameters via a superconducting transmission line to which the said superconducting thermal detector (bolometer) of any of paragraphs 1) to 7) is coupled either via a capacitance or via an inductance or via a circuit containing both an inductance and a capacitance. The bolometer array circuit comprising linear or 2-dimensional matrix of superconducting thermal defectors
(bolometers) consists of individual bolometer resonant circuits with different resonant frequencies coupled to a superconducting transmission line via a capacitance or via an inductance or via a circuit containing both inductive and a capacitive elements.
DISCLAIMER
Although the theoretical description described herein is thought to be correct, the operation of the devices/detectors described here does not depend upon the accuracy or validity of the theoretical description. That is, latter theoretical developments that may explain the observed results on a basis different from the theory presented herein will not detract from the inventions described herein.
Any patent, patent application, or publication identified in the specification is hereby incorporated by reference herein in its entirety. Any material, or portion thereof, that is said to be incorporated by reference herein, but which conflicts with existing definitions, statements, or other disclosure material explicitly set forth herein is only incorporated to the extent that no conflict arises between the incorporated material and the present disclosure material, in the event of a conflict, the conflict has to be resolved in favour of present disclosure as the preferred disclosure.
While the present invention has been particularly shown and described with reference to the preferred mode as illustrated in the drawing, it will be understood by one skilled in the art that various changes in detail may be affected therein without departing from the spirit and scope of the invention as defined by the claims.
C!TED PATEiSST DOCUMENT
D,G. McDonald, U.S. Patent No, 4,889,598, issued Sep. 26 1989.
REFERENCES AND RELATED UTERATURE
[1] D.H. Andrews, Yearbook - Am. Philos. Soc. (1938), 132.
A. Goetz, Phys. Rev. 55, 1270, 1939.
D.H, Arsdre s et a!., Phys, Rev. 59, 1045, 1941,
[2] D.G. McDonald, Applied Physics Letters, VoL 50, p. 775, 1987.
D.G. IvkDoriald, SEEE Traris. on Magnetics, VoL 25, No. 2, 1989.
[3] E.N. Grossmars, D.G. McDona!d and J. E. Sauvageau,
!EEE Trans. Oil fvlagiietics, Vol. 27, No, 2, IVlarch 1991, 2677-2680; 2757-2760.
[4] P, . Day et aL, Nature, VoL 425, p. 817, 2003. R. Barends, Ph.D. thesis, Delft University of Technology, 2009.
Doyle et al, 32" international Conference on infrared and IVliii
! pp. 450-451, 2007.
[7] Jonas Zmuidzinas, Ann. Rev. Condens. Matte Phys. 2012. 3:169-214. A: A millimeter- kinetic inductance camera,
A. ini et aL, Astronomy arsd Physics, Vol 521, Oct 2010,
[9] IVIAKQ: a pathfinder instrument for on-sky demonstration of k
imaging arrays, toren^J^ Swenson,, et ai, Proc, SPSE 8452, Miinmeter, SubmiiHmeter, and Far- !nfrared Detectors and instrumentation for Astronomy Vi,
doi:10.1117/12.926223.
Figure imgf000021_0001
[11] Duai- !arization sensitive M !Ds for far-infrared astrophysics, J. Hubmayr et a!, ASC ors App!ied Superconductivity, ta!k 5EB-06.
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[13] N. Vercruyssen et aL, Appl. Phys. Lett. 99, 062509 (2011).

Claims

What is claimed is:
1) A superconducting thermal detector (bolometer) including
a. an absorbing element (1) for absorbing electromagnetic (THz) radiation, b. a thermally isolated from a substrate (3) superconducting inductive element
(2) in thermal contact with the radiation absorbing element (1), and c. a read-out circuit (4) for indicating the absorbed electromagnetic (THz) radiation,
characterized in that
d. the superconducting inductive element (2) is thermally isolated by insulator layer (5) micro-suspensions (11),
e. the superconducting inductive element (2) is electrically connected to a capacitor (Csh) in order to form a resonator circuit (Csh, 2), and f. the read-out circuit (4) is implemented by sensing the change in amplitude or phase or both changes in amplitude and in phase of the resonator circuit (Csh,
2).
2) A superconducting thermal detector (bolometer) in accordance with claim 1), characterized in that the superconducting inductor phonon system is located on the membrane (5), whereas the said membrane (5) is thermally isolated from the phonon system of the substrate (3) by micro-suspensions (11).
3) A superconducting thermal detector (bolometer) in accordance with claims 1) or 2), characterized in that the said superconducting inductive element (2) comprises a superconducting material having a high normal state resistivity.
4) A superconducting thermal detector (bolometer) in accordance with claims 1) or 2), characterized in that the said superconducting inductor comprises a superconducting material such as Aluminium (Al), Niobium (Nb), Vanadium (V), Tungsten silicide (WSi), Magnesium diboride (MgB2) or other-like superconducting material having superconducting transition temperatures in temperature range 1 Kelvin - 20 Kelvin.
5) A superconducting thermal detector (bolometer) in accordance with claims 1) or 2), characterized in that the said superconducting inductor comprises a superconducting material comprising nitrogen (N) and a metal selected form the group consisting of Niobium (Nb), Titanium (Ti) and Vanadium (V).
6) A superconducting thermal detector (bolometer) in accordance with any of previous claims 1) - 5) characterized by utilizing kinetic inductance thermometry which is read out by a scattering parameter measurement which can be used to determine the amplitude or phase change in the resonator induced by impinging optical (THz) power.
7) A superconducting thermal detector (bolometer) in accordance with any of previous claims 1) - 6), characterized in that it utilizes kinetic inductance thermometry and incorporates an impedance matching surface for efficient absorption of incident optical (THz) power.
8) A superconducting thermal detector (bolometer) in accordance with any of previous claims 1) - 7), characterized in that it utilizes kinetic inductance thermometry and incorporates an antenna and an antenna termination which dissipates the incident optical (THz) power and translates it to heat to be sensed by the kinetic inductance thermometer.
9) A read-out circuit (4) of incident THz radiation signal characterized in that it is implemented by sensing microwave transmission/reflection parameters via a superconducting transmission line to which the superconducting thermal detector (bolometer) in accordance with any of claims 1) to 8) is coupled either via a capacitance or via an inductance or via a circuit containing both inductive and capacitive elements.
10) A bolometer array in accordance with any of previous claims 1) - 9) characterized in that it comprises linear or 2-dimensional matrix of the superconducting thermal detectors (bolometers) comprising individual bolometer resonant circuits with different resonant frequencies coupled to a superconducting transmission line by either via a capacitance or via an inductance or via a circuit containing both inductive and capacitive elements.
11) A method for manufacturing a superconducting thermal detector (bolometer) characterized in that it comprises the following steps: deposition of a membrane layer (5) onto a silicon substrate (3),
deposition of superconducting inductor layer (6) over the membrane layer (5) by sputtering method in argon atmosphere,
deposition of insulator layer (7) over the superconducting inductor layer (6), deposition of absorber layer (1) over the insulator layer (7) followed by wet etching or by dry etching to form absorbing element (1), e. forming micro-suspensions (11) in order to isolate thermally the part of the superconducting inductor layer (6) forming superconducting inductive element (2) from the substrate (3).
12) A method in accordance with claim 11, characterized by deep etching of silicon to release the membrane layer (5) by anisotropic silicon ICP etching or by wet etching.
13) A method in accordance with any previous method claim, characterized by deposition of etch-stop layer such as silicon oxide or onto a silicon substrate (3).
14) A method in accordance with any previous method claim, characterized in that the membrane layer (5) comprises a 100 nm to 1 μιη thick film of a material such as a silicon nitride (SiN, Si3N4), a silicon oxide (SiO, Si02), or other-like materials used to form membranes.
15) A method in accordance with any previous method claim, characterized in that the superconducting inductor (6) comprises a 3 nm to 500 nm thick film of a superconducting material such as niobium (Nb), niobium nitride (NbN) or niobium titanium nitride (NbTiN) and that the material of superconducting inductor layer 6 is selected from the following: Nb, NbN, or NbTiN, and other superconducting materials such as aluminium (Al), vanadium (V), vanadium nitride (VN), tungsten silicide (WSi), magnesium diboride (MgB2) and other-like are used.
16) A method in accordance with any previous method claim, characterized in that the superconducting inductor layer (6) is patterned by micro-lithography and by wet etching or by plasma etching.
17) A method in accordance with any previous method claim, characterized in that the insulator layer (7) material comprises a 10 nm to 1 μιη thick film of silicon nitride (SiN, Si3N4), a silicon oxide (SiO, Si02), aluminium oxide (AIO, Al203), or other-like insulator materials.
18) A method in accordance with any previous method claim, characterized in that the insulator layer (7) is patterned by micro-lithography and by wet etching or by plasma etching.
19) A method in accordance with any previous method claim, characterized by deposition of 2nd superconducting layer (8) comprising a 3 nm to 1 μιη thick film comprising any of superconducting materials listed in the step 3 of deposition of superconducting inductor layer (6). 20) A method in accordance with any previous method claim, characterized in that the 2nd superconducting layer (8) is patterned by micro-lithography and by wet etching or by plasma etching
21) A method in accordance with any previous method claim, characterized in that the material of an absorbing element ()1 comprises a normal metal 100 nm thick film of titanium tungsten (TiW) and the material of absorbing element (1) is selected from TiW, and other metallic materials such as Mo, Ti and the like to form the absorbing element (1).
22) A method in accordance with any previous method claim, characterized in forming membrane perforations (21) and micro-suspension legs (11) to enhance thermal isolation of a superconducting inductor (2) or/and absorbing element (1) .
23) A method in accordance with any previous method claim, characterized in that the perforations (21) in the membrane layer (5) are patterned by micro-lithography and by wet etching or by plasma etching.
24) A method in accordance with any previous method claim, characterized in that in order to enhance absorption of THz radiation, an optical cavity (9) of a gap of 2/4 or odd multiples of 2/4: (2n+ 1)^ (n = l,2, . . . ) in formed between an absorbing element (1) and the attached back reflector (10).
25) A method in accordance with any previous method claim, characterized in forming 2/4 ~ 214 μιη or 32/4 ~ 643 μιη or optical cavity (the wavelength 2 ~ 857 μτη for incoming 350 GHz radiation) the silicon wafer substrates (3) with corresponding approximate thicknesses of 2/4 and 32/4 are used in the microfabrication process of a superconducting thermal detector (bolometer.
26) A method in accordance with any previous method claim, characterized in that the back reflector (10) comprises a reflective surface or a reflective film deposited onto another substrate, which are attached to the substrate (3).
27) A method in accordance with any previous method claim, characterized in removing etch-stop silicon oxide layer in a buffered HF solution or in a dry HF vapour etcher.
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